منابع مشابه
Preparative isolation and purification of coumarins from Peucedanum praeruptorum Dunn by high-speed counter-current chromatography.
A preparative high-speed counter-current chromatography (HSCCC) method for isolation and purification of coumarins from Peucedanum praeruptorum Dunn (Baihuaqianhu in Chinese) was successfully established by using light petroleum-ethyl acetate-methanol-water as the two-phase solvent system in gradient elution mode. The upper phase of light petroleum-ethyl acetate-methanol-water (5:5:5:5, v/v) wa...
متن کاملCoumarins and a naphthyl labdanoate diarabinoside from the fruits of Peucedanum grande C. B. Clarke.
Phytochemical investigations of the methanolic extract of the fruits of Peucedanum grande C. B. Clarke (Apiaceae) led to the identification of three coumarins and a naphthyl labdanoate diarabinoside characterized as 5-hydroxy-6-isopranyl coumarin (1), 5,6-furanocoumarin (2), 7-methoxy-5,6-furanocoumarin (3), and labdanyl-3alpha-ol-18-(3'"-methoxy-2"'-naphthyl-oate)-3alpha-L-arabinofuranosyl-(2'...
متن کاملSynthesis of Functionalized Coumarins
The synthesis of functionalized 2-oxo-2H-coumarin derivatives has been studied by a one-pot reaction of o-hydroxybenzaldehyde, ethyl 2-bromoacetate and triphenylphosphine in the presence of catalytic amount of triethyl amine in EtOAc, water or under solvent free conditions. We have found the best results obtained under solvent free condition.
متن کاملFuranocoumarins from Peucedanum Tauricum Bieb
A rapid and sensitive reversed-phase high-performance liquid chromatographic (RP-HPLC) method has been used for determination of furanocoumarins in methanolic extracts of Peucedanum tauricum Bieb. HPLC separation was performed on a C18 analytical column (250 mm × 4 mm i.d., 5-μm particles) with a methanol–water gradient as mobile phase. A second chromatographic system with an acetonitrile–water...
متن کاملSupramolecular photodimerization of coumarins.
Stereoselective photodimerization of coumarin and its derivatives in supra-molecular systems is reviewed. The enantioselective photodimerization of coumarin and thiocoumarin in inclusion crystals with optically active host compounds is also described.
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ژورنال
عنوان ژورنال: Chemistry of Natural Compounds
سال: 1975
ISSN: 0009-3130,1573-8388
DOI: 10.1007/bf00571232